SPELEC UV-VIS Instrument (200-900 nm) for Spectroelectrochemical Measurement

SPELEC is a tool for spectroelectrochemical measurements. It comprises a spectrometer (UV-VIS wavelength range: 200-900 nm), a bipotentiostat/galvanostat, and a lightsource in one box.

It also comes with specialized spectroelectrochemical software that enables the synchronization of optical and electrochemical studies.

Tech Specs

Source: Metrohm USA Inc.

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Operating modes Bipotentiostat; Potentiostat; Galvanostat
PC interface USB
Power 12 V DC
Potential range in volt ±4 V
Maximum current in Ampère ±40 mA
Number of current ranges 8
Number of current ranges remarks ±1 nA to ±10 mA
Number of potential ranges (galvanostat) 2
Number of potential ranges remarks (galvanostat) ±100 mV to ±1 V
Multichannel instrument NO
Maximum number of channels 1
Maximum number of WE sharing AUX and REF 2
Potential accuracy ±0.2%
Current accuracy ≤0.5% of current range at 100 nA to 10 mA
Potential resolution 1 mV
Current resolution 0.1% of current output range
Measured potential resolution 0.012% of potential range
Measured current resolution 0.025% of current range
Spectrometer (SPM) Detector Linear silicon CCD array
SPM Pixels 2048
SPM Pixel size 14 µm x 200 µm
SPM Pixel well depth 62,500 electrons
SPM Wavelength range 200-900 nm
SPM Optical resolution 0.3+10.0 nm FWHM
SPM Signal-to-noise ratio 250:1 (at full signal)
SPM A/D resolution 16 bit
SPM Dark noise 50 RMS counts
SPM Dynamic range 8.5 x 10 rised to 7 (system) ; 1300:1 for a single acquisition
SPM Integration time 1 ms to 65 seconds
SPM Stray light ≤ 0.05% at 600 nm ; < 0.10% at 435 nm
Light Source (LS) wavelength range 215-400 nm (deuterium) ; 360-2500 nm (tungsten halogen)
LS Stability 1.0% peak-to-peak (over 4 hours) after 30-minute warm-up
LS Time to stable output 10 minutes (deuterium) ; 1 minute (tungsten halogen)
LS Ignition delay <2.0 seconds (delay for cold start-up may be longer)
LS Bulb life >1,000 hours @ 240 nm (time); <50% @ 240 nm (decrease of intensity) ; Continuous operation (testing conditions)
LS Fiber optic connector SMA 905
Dimensions 24 x 11 x 25
Weight of the instrument in kg 1.95

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