SPELEC is a tool for spectroelectrochemical measurements. It comprises a spectrometer (UV-VIS wavelength range: 200-900 nm), a bipotentiostat/galvanostat, and a lightsource in one box.
It also comes with specialized spectroelectrochemical software that enables the synchronization of optical and electrochemical studies.
Tech Specs
Source: Metrohm USA Inc.
. |
. |
Operating modes |
Bipotentiostat; Potentiostat; Galvanostat |
PC interface |
USB |
Power |
12 V DC |
Potential range in volt |
±4 V |
Maximum current in Ampère |
±40 mA |
Number of current ranges |
8 |
Number of current ranges remarks |
±1 nA to ±10 mA |
Number of potential ranges (galvanostat) |
2 |
Number of potential ranges remarks (galvanostat) |
±100 mV to ±1 V |
Multichannel instrument |
NO |
Maximum number of channels |
1 |
Maximum number of WE sharing AUX and REF |
2 |
Potential accuracy |
±0.2% |
Current accuracy |
≤0.5% of current range at 100 nA to 10 mA |
Potential resolution |
1 mV |
Current resolution |
0.1% of current output range |
Measured potential resolution |
0.012% of potential range |
Measured current resolution |
0.025% of current range |
Spectrometer (SPM) Detector |
Linear silicon CCD array |
SPM Pixels |
2048 |
SPM Pixel size |
14 µm x 200 µm |
SPM Pixel well depth |
62,500 electrons |
SPM Wavelength range |
200-900 nm |
SPM Optical resolution |
0.3+10.0 nm FWHM |
SPM Signal-to-noise ratio |
250:1 (at full signal) |
SPM A/D resolution |
16 bit |
SPM Dark noise |
50 RMS counts |
SPM Dynamic range |
8.5 x 10 rised to 7 (system) ; 1300:1 for a single acquisition |
SPM Integration time |
1 ms to 65 seconds |
SPM Stray light |
≤ 0.05% at 600 nm ; < 0.10% at 435 nm |
Light Source (LS) wavelength range |
215-400 nm (deuterium) ; 360-2500 nm (tungsten halogen) |
LS Stability |
1.0% peak-to-peak (over 4 hours) after 30-minute warm-up |
LS Time to stable output |
10 minutes (deuterium) ; 1 minute (tungsten halogen) |
LS Ignition delay |
<2.0 seconds (delay for cold start-up may be longer) |
LS Bulb life |
>1,000 hours @ 240 nm (time); <50% @ 240 nm (decrease of intensity) ; Continuous operation (testing conditions) |
LS Fiber optic connector |
SMA 905 |
Dimensions |
24 x 11 x 25 |
Weight of the instrument in kg |
1.95 |